岩石显微构造分析现代技术——EBSD技术及应用   总被引：10，自引：0，他引：10  

曹淑云  刘俊来 《地球科学进展》2006,21(10):1091-1096

EBSD技术的发展，为岩石显微构造分析开辟了一个全新的领域。它与现代扫描电子显微镜和能谱分析等设备配合，可以同时对块状样品进行晶体结构与成分分析,从而使显微构造、微区成分与结晶学数据分析有机结合起来。 EBSD技术可以精确、快速定量标定包括各种晶系晶体颗粒的晶格方位和描述晶体颗粒的边界、形态等特征，对于具有低角度边界的晶体颗粒提供精确数据,为阐述岩石变形机制提供重要约束，并为高级晶族和不透明矿物结晶学组构与变形机制研究提供了有效的手段。EBSD尤其使获取微米级甚至纳米级尺度上颗粒（亚颗粒）或相之间的定向差别（达到20 nm的空间分辨率和0.3度角度分辨率）成为可能。EBSD技术在矿物相鉴定、亚微域内的应变分析、矿物出溶作用等方面的应用，进一步证明了这一新技术在显微构造分析及相关领域的应用前景。其广泛应用必将带来岩石显微构造研究的新突破，也将成为未来岩石变形机制与岩石圈流变学研究取得飞速发展不可或缺的技术手段。  相似文献   

The structure of the mid- and high-latitude ionosphere during the November 2004 storm event obtained from GPS observations   总被引：1，自引：1，他引：1  

Andrzej Krankowski  Irk I. Shagimuratov  Lubomir W. Baran  Galina Yakimova 《Acta Geophysica》2007,55(4):490-508

GPS data from the International GNSS Service (IGS) network were used to study the development of the severe geomagnetic storm of November 7–12, 2004, in the total electron content (TEC) on a global scale. The TEC maps were produced for analyzing the storm. For producing the maps over European and North American sectors, GPS measurements from more than 100 stations were used. The dense network of GPS stations provided TEC measurements with a high temporal and spatial resolution. To present the temporal and spatial variation of TEC during the storm, differential TEC maps relative to a quiet day (November 6, 2004) were created. The features of geomagnetic storm attributed to the complex development of ionospheric storm depend on latitude, longitude and local time. The positive, as well as negative effects were detected in TEC variations as a consequence of the evolution of the geomagnetic storm. The maximal effect was registered in the subauroral/auroral ionosphere during substorm activity in the evening and night period. The latitudinal profiles obtained from TEC maps for Europe gave rise to the storm-time dynamic of the ionospheric trough, which was detected on November 7 and 9 at latitudes below 50°N. In the report, features of the response of TEC to the storm for European and North American sectors are analyzed.  相似文献   

From geometry to dynamics of microstructure: using boundary lengths to quantify boundary misorientations and anisotropy   总被引：1，自引：0，他引：1  

John Wheeler  Z. Jiang  D. J. Prior  J. Tullis  M. R. Drury  P. W. Trimby 《Tectonophysics》2003,376(1-2):19-35

The microstructure of a quartzite experimentally deformed and partially recrystallised at 900 °C, 1.2 GPa confining pressure and strain rate 10⁻⁶/s was investigated using orientation contrast and electron backscatter diffraction (EBSD). Boundaries between misoriented domains (grains or subgrains) were determined by image analysis of orientation contrast images. In each domain, EBSD measurements gave the complete quartz lattice orientation and enabled calculation of misorientation angles across every domain boundary. Results are analysed in terms of the boundary density, which for any range of misorientations is the boundary length for that range divided by image area. This allows a more direct comparison of misorientation statistics between different parts of a sample than does a treatment in terms of boundary number.The strain in the quartzite sample is heterogeneous. A 100×150 μm low-strain partially recrystallised subarea C was compared with a high-strain completely recrystallised subarea E. The density of high-angle (>10°) boundaries in E is roughly double that in C, reflecting the greater degree of recrystallisation. Low-angle boundaries in C and E are produced by subgrain rotation. In the low-angle range 0–10° boundary densities in both C and E show an exponential decrease with increasing misorientation. The densities scale with exp(−θ/λ) where λ is approximately 2° in C and 1° in E; in other words, E has a comparative dearth of boundaries in the 8–10° range. We explain this dearth in terms of mobile high-angle boundaries sweeping through and consuming low-angle boundaries as the latter increase misorientation through time. In E, the density of high-angle boundaries is larger than in C, so this sweeping would have been more efficient and could explain the relative paucity of 8–10° boundaries.The boundary density can be generalised to a directional property that gives the degree of anisotropy of the boundary network and its preferred orientation. Despite the imposed strain, the analysed samples show that boundaries are not, on average, strongly aligned. This is a function of the strong sinuosity of high-angle boundaries, caused by grain boundary migration. Low-angle boundaries might be expected, on average, to be aligned in relation to imposed strain but this is not found.Boundary densities and their generalisation in terms of directional properties provide objective measures of microstructure. In this study the patterns they show are interpreted in terms of combined subgrain rotation and migration recrystallisation, but it may be that other microstructural processes give distinctive patterns when analysed in this fashion.  相似文献   

Crystallographic orientations of high-angle grain boundaries in dynamically recrystallized quartz: First results   总被引：1，自引：0，他引：1  

Boriana Kuntcheva  Jrn H. Kruhl  Karsten Kunze 《Tectonophysics》2006,421(3-4):331-346

The crystallography and geometry of high-angle grain boundaries from dynamically recrystallized quartz have been studied. On the basis of combined electron backscatter diffraction and universal stage measurements, the complete crystallographic orientation of the grain boundaries could be calculated. The u-stage rotation of the grain boundaries to a vertical position reveals that they are never curved but always consist of straight segments. Our results show that these segments preferentially occupy rhombohedral, trapezohedral and bipyramidal orientations, i.e., orientations in a  25–50° girdle to the c-axis. A specific, albeit low, number of segments with special crystallographic orientation, with respect to a neighbouring quartz grain, often shows another special orientation with respect to the other neighbouring grain. Preferred combinations of grain boundary orientations related to both neighbouring grains are (i) low-index rhombohedral and high index trapezohedral, (ii) low-index bipyramidal and low-index trapezohedral or high-index rhombohedral, and (iii) low-index trapezohedral and low or high index trapezohedral. In certain cases, such as at triple junctions, the boundaries occupy specific trapezohedral orientations with a constant angle to the c-axis. This argues for energy isotropy of trapezohedral planes with the same angle to the quartz c-axis. In general, good match coincidence site lattice (CSL) orientations are not preferentially occupied so that most of the studied grain boundaries represent general boundaries. The formation of straight segments in special crystallographic orientations indicates the crystallographic control and implies an energy reduction of certain general boundaries.  相似文献   

冲绳海槽玄武岩中中酸性残余熔体研究及其岩石学意义   总被引：1，自引：0，他引：1  

陈小明  王汝成赵明 倪培赵广涛  李巍然 《岩石学报》2005,21(1):158-168

与洋壳有关的酸性岩由于对了解幔源岩浆的演化以及判别古老蛇绿岩套及其构造位置的重要意义而倍受岩石学家和构造地质学家的关注。本对发现于冲绳海槽玄武岩基质中的中酸性到酸性残余熔体进行了详细研究，它们提供了幔源玄武岩浆结晶分异形成酸性岩浆的直接证据。在细小的基质矿物间分布有一种玻璃质的残余熔体，其成分随距冷凝边距离(L)的增加而越来越酸性。在SiO2对Na2O K2O图解上，残余熔体的投影点从玄武岩到英安岩均有分布，反映了一个连续的演化系列。在AFM图解上，残余熔体表现出与Thingmuli火山岩系列类似的拉斑玄武岩系列的演化趋势。我们的研究表明：残余熔体的演化受结晶分异作用控制。在早期结晶阶段，辉石的结晶起主导作用，结果造成残余熔体中SiO2、Al2O3，Na2O的迅速增加，FeO、MgO、CaO迅速降低。在晚期结晶阶段，斜长石成为主导结晶相，导致残余熔体中Al2O3，Na2O的迅速消减。Al2O3、Na2O从增加到降低的转变出现在SiO2=62％左右。在L=27．5mm处，85～90％的基质岩浆已发生了结晶作用，导致残余熔体中SiO2含量达到69～70％，而且此处还新出现了一种富FeTi的氧化物。该玄武岩中残余熔体和基质矿物的成分及演化特征分别与Thingmuli火山岩系列中酸性端元的组成相似，在也佐证了Thingmuli火山岩系列是幔源岩浆结晶分异的产物.  相似文献   

Defect structure of the low temperature α-cristobalite phase and the cristobalite ⇆ tridymite transformation in (Si-Ge)O2     

H. Lemmens  M. Czank  G. Van Tendeloo  S. Amelinckx 《Physics and Chemistry of Minerals》2000,27(6):386-397

Using minimum exposure techniques, it is feasible to perform high resolution electron microscopy on the α-cristobalite phase of (Si_0.9 Ge_0.1)O₂, which is extremely radiation sensitive. Such images reveal atomic scale information of twins and tridymite-like stacking faults on (1 1 1)_β planes, as well as of domain boundaries resulting from the β→α transition. Polytype structures are formed in certain cases. Morphological features suggest that the phase transformation cristobalite → tridymite proceeds by means of a zonal dislocation mediated synchro-shear process on (1 1 1)_β planes; the geometry of this process is analyzed. Received: 13 June 1999 / Accepted: 30 October 1999  相似文献   

颅颌面外科与三维重建技术   总被引：16，自引：1，他引：15  

归来  戴汝平 《CT理论与应用研究》2000,9(3):31-34

目的 探讨电子束ＣＴ三维重建技术在颅颌面外科的适应症和应用价值。方法 采用美国Ｉｍａｔｒｏｎ公司的电子束ＣＴ（ｅｌｅｃｔｒｏｎ ｂｅａｍ ＣＴ,以下简称ＥＢＣＴ）Ｃ－１５０,对７６例严重颅颌面病人实行薄层ＣＴ容积扫描。将所获ＣＴ 象经数字接口传至加拿大ＩＳＧ公司生产的Ａｌｌｅｇｒｏ工作站进行三维重建。结果 ＥＢＣＴ成像技术能立体的、详尽和精确的显示机体组织三维解剖结构极其相互关系。其再现畸形或病体  相似文献   

工业CT技术在卫星产品检测中的应用   总被引：2，自引：0，他引：2  

倪培君  李旭东  梁晓明  王爱华  孙守黑 《CT理论与应用研究》2000,9(Z1):119-123

卫星产品许多都采用了焊接结构。为了保证其使用的安全可靠性,必须对焊缝进行l00％的无损检测。然而对于一些形状复杂的精密电子束焊件,由于产品尺寸小,加之焊缝周围结构的遮挡,使常规方法的应用受到了限制。工业CT技术具有不受试件材料种类、形状结构及表面状况限制的特点,能给出与试件材料密度及尺寸特性相对应的断层扫描图象,分辨率高,在检测复杂构件方面显示出了优势。本文介绍了卫星产品精密复杂焊接件对无损检测技术的具体要求,研究了卫星产品电子束焊缝的工业CT检测方法,包括设备、对比试样、检测工艺、评定方法等,并通过电磁阀、喷注器、自锁阀、减压器、加注/排放阀、单向阀、气滤、过滤器等具体产品检测实例,描述了工业CT技术在卫星产品检测中的应用。实际应用表明：工业CT是检测航天卫星产品精密复杂结构件焊缝缺陷的理想手段,其成象直观,缺陷的定位、定性和定量结果可靠,完全能满足产品的质量控制要求。目前,累计用工业CT检测卫星产品数批若干件,检测焊缝上千条。剔出有超标缺陷的产品40件,避免了隐患。经过工业CT检测的产品,己在"返回式卫星"、"风云二号"、"东方红三号"、"资源一号"、"中星-22号"等型号卫星中取得了成功应用。  相似文献   

用电子束CT作冠状动脉血管造影     

Stephan Achenbach  Dieter Ropers  Werner G. Daniel  Werner Moshage 《CT理论与应用研究》2000,9(1):45-48

本文介绍用电子束ＣＴ作冠状动脉可视化造影的方法,说明本项成就的特征和在应用这项技术的局限性,并指出这种技术在临床上,可能成为新无创伤性的诊断工具。  相似文献   

Characteristics and genesis of maghemite in Chinese loess and paleosols: Mechanism for magnetic susceptibility enhancement in paleosols   总被引：4，自引：0，他引：4  

Tianhu Chen  Huifang Xu  Qiaoqin Xie  Jun Chen  Junfeng Ji  Huayu Lu 《Earth and Planetary Science Letters》2005,240(3-4):790-802

Morphological characteristics and microstructures of magnetic minerals extracted from Chinese loess and paleosols were investigated using powder X-ray diffraction (XRD) and high-resolution transmission electron microscopy (HRTEM). Our results indicate that maghemite in loess–paleosol sequences was transformed from magnetite through oxidation of magnetite. Maghemite transformed from eolian magnetite during chemical weathering has low-angle grain boundaries among maghemite nano-crystals. Some nano-crystalline maghemites with nanoporous texture resulted from microbe-induced precipitation of magnetite or transformation of poorly crystalline ferric Fe (oxy)hydroxides in presence of Fe-reducing bacteria. Aggregates of euhedral maghemite nano-crystals were transformed from magnetite magnetosomes. Both microbe-induced nanoporous magnetite and microbe-produced magnetite magnetosomes are directly related to microbial activities and pedogenesis of the paleosols. It is proposed that the formation of nano-crystalline maghemite with superparamagnetic property in paleosol results in the enhancement of magnetic susceptibility, although the total amount (weight percent) of magnetic minerals in both paleosol and loess units is similar. Our results also show that nano-crystalline and nanoporous magnetite grains prefer to transform into maghemite in semi-arid soil environments instead of hematite, although hematite is a thermodynamically stable phase. This result also indicates that a decrease in crystal size will increase stability of maghemite. It is also inferred that surface energy of maghemite is lower than that of hematite.  相似文献